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Ref. No. [UMCES] CBL 2015-011

ACT VS15-04

17

As defined in the test protocols, two Metrohm electrodes were maintained within the test

tank throughout the lab study to provide a continuous, independent measure of pH at 15 minute

intervals. These results were not intended to be used as reference values for direct instrument

comparison, but because they were calibrated weekly with water from the test tank water against

the dye reference pH and they maintained their calibration in between intervals (Fig. 2; slope =

1.006, r

2

= 0.999), they provide a high resolution (15 minute) continuous time series of ambient

pH within the test tank. Therefore, Metrohm results are included within some of the time series

plots but no quantification of instrument accuracy was conducted with these data.

Figure 2.

Cross plot of matched Metrohm pH results that measured continuously within the test tank at

15 minute intervals versus dye measured reference pH results. Three-hundred, fifty-one dye based pH

measurements were made over the ten week test.