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Ref. No. [UMCES] CBL 2015-008

ACT VS15-01

50

Table 7.

Results of Field Duplicates (FD) and Field Trip Blank (FTB) for the Great Lakes, MI mooring

test. The field trip blank was determined with a mixture of commercial NBS buffers.

Date/Time

Rep

Temp

Salinity

pH

Std Dev Mean Std Dev

ABS

Diff

6-23-14 11:15

FD1

19.7

0.029

8.013

.003

8.016

.004

.005

FD2

8.018

.003

6-27-14 14:30

FD1

21.0

0.030

8.324

.004

8.322

.002

.003

FD2

8.321

.008

7-8-14 10:15

FD1

21.1

0.031

8.136

.001

8.131

.008

.011

FD2

8.125

.004

7-10-14 12:00

FD1

21.0

0.031

8.387

.010

8.400

.018

.025

FD2

8.412

.006

7-17-14 15:15

FD1

20.4

0.032

8.304

.008

8.300

.006

.009

FD2

8.295

.007

7-19-14 10:15

FD1

20.4

0.032

8.275

.002

8.273

.003

.004

FD2

8.271

.008

7-14-14 9:15

FTB1

22.0

0.032

8.258

.005

8.257

.002

.003

FTB2

8.255

.003

External Quality Assurance and Quality Control Assessments

An effective assessment program is an integral part of ACT’s quality system for

performance evaluations of marine sensor technologies. The ACT Quality Assurance (QA)

Manager independently conducted three technical systems audits (TSA), an audit of data quality

(ADQ), and a Data Quality Assessment (DQA) for the pH verification. The audits were

conducted in accordance with the procedures described in EPA's

Guidance on Technical Audits

and Related Assessments for Environmental Data Operations (EPA QA/G-7)

.

Technical System Audit -

A Technical Systems Audit (TSA) is a thorough, systematic, on-site

qualitative audit of ACT’s sampling and measurement processes and procedures associated with

a specific technology verification. The objective of a TSA is to assess and document the

conformance of on-site testing procedures with the requirements of the Test Protocols, and

associated SOPs. The ACT QA Manager conducted the following three TSAs over the course of

the verification:

The laboratory tests at the Hawai‘i Institute of Marine Biology (HIMB), Coconut

Island, Kaneohe Bay, Oahu, HI during December 11-15, 2012.

The field tests at HIMB during November 19-21, 2013.

The field tests at the Chesapeake Biological Laboratory, Solomons, MD during

March 11-14, 2014